The removal of carbon dioxide from beer in preparation for analysis.
The removal of carbon dioxide from beer in preparation for analysis.
This method specifies a high performance liquid chromatographic technique for the simultaneous determination of iso-α-acids (Iso) and reduced iso-α-acids (Rho, Tetra and Hexa) in beer. Due to coelution of Hexa and Iso peaks, this method is not recommended for the analysis of beers containing mixtures of Hexa and Iso compounds.
Determination of the N-Nitrosodimethylamine (NDMA) content of beer.
It is necessary to use EBC Method 4.1
The determination of selected hop-derived aroma components (myrcene, linalool, geraniol, 2-methylbutyl isobutanoate) in beer by automatic headspace-trap gas chromatography in combination with mass spectrometry.
It is necessary to use EBC Method 9.46
This method specifies a high performance liquid chromatographic technique for the simultaneous determination of iso-α-acids (Iso), humulinones (Hum) and α-acids (Alpha) in beer. It is recommended for dry hopped beers containing humulinones (and α-acids) in addition to iso-α-acids. Due to coelution of humulinones (or α-acids) and reduced iso-α-acids (Rho, Tetra, Hexa, see method EBC 9.47.1), this method is not recommended for the analysis of beers containg reduced iso-α-acids. This method was validated for the determination of humulinones and iso-α-acids in beer. The method is not a validated method for determination of α-acids , but can be used as a guideline method for the determination of α-acids
This section describes general techniques for taking and preparing samples of a solid process aid for use in conjunction with a previously established sampling plan.
It is necessary to use EBC Method 3.1
The determination of the moisture content of solid process aids using a loss in mass on drying under specified conditions. Descriptors: mass of process aid before drying in g, mass of process aid after drying in g, moisture content of the process
The determination of the degree of calcination of powders and sheets used for filtration by heating in a furnace. Descriptors: Calcination loss expressed as a percentage of the dry material, Mass of dry filter aid before calcination g, Mass of sample after calcination g.
It is necessary to use EBC Methods 10.1 and 10.2
The determination of the volume occupied by a fixed mass of filter aid. This data is particularly important for the assessment of new filter aids in a filtration process. Descriptors: density of the filter bed (g/ml), volume of the filter bed after sedimentation (ml), mass of sample (g)
Determination of the pH of an aqueous suspension of filter aids.
It is necessary to use EBC Methods 8.17 and 10.1
The determination of the soluble iron content of solid process aids by extraction with a buffer solution or beer. Descriptors: soluble iron content of the process aid in mg/kg, iron content of the test filtrate, in mg/litre, iron content of the blank filtrate, in mg/litre, m is the mean value, in mg/kg.
It is necessary to use EBC Methods 10.1 and 9.13.1 or 9.13.2 or 9.13.3
For the approval of new materials or new suppliers by evaluating the sensory impact of process aids on the aroma and taste of beer. For use within problem solving related to off-flavours or taints.
It is necessary to use EBC Methods 10.1, 13.3, 13.4 and 13.14
The determination of the permeability which is a principal characteristic of filter aids. Descriptors: Operating Conditions, Permeability expressed in Darcy units, Conversion factor for units, Volume filtered in ml, Filter cake height in cm, thickness of the wet filter sheet, viscosity of water, Surface of filtration, Filtration pressure in bar, flow time in s.
The determination of filtration rate and permeability of filter aids, using the EBC filter unit.
It is necessary to use EBC Methods 10.1 and 10.8
The determination of the mass per unit of surface area and the thickness of filter sheets, which are characteristic for different types of sheet.
For the approval of new gases or new suppliers of gases for use in brewing or packaging by evaluating their potential to taint the aroma and taste of water, wort or beer. For use within problem solving related to off-flavours or taints.
It is necessary to use EBC Methods 13.4 and 13.14
A simple practical means of sampling bottles for performing such tests as visual inspection of glass bottles, dimensional examination and glass weight.
It is necessary to use
The determination of the amount of air in the headspace of bottles and cans using a "funnel" method.
A rapid method for determining the amount of headspace and total gases other than carbon dioxide in a container. The proportion of oxygen contained in these gases does not always correspond to the natural proportion of airborne oxygen, but can be bigger or smaller. In fresh filled beer samples it is usually between the 10 % and 30 % (nitrogen between 90 % and 70 %). Descriptors: volume of gas in ml, nominal volume of beer in container in ml.
It is necessary to use EBC Method 9.28.3
The determination of the net content of bottles and cans by weighing. The derivation of volume from weight has the advantage, aside from the higher accuracy, that the temperature of individual packages do not have to be taken into account. The specific gravity, however, must be measured at 20 ºC. Descriptors: weight of the full unopened container, weight of the empty container or tare weight, a is the CO2 content % (m/m) of the beer.
It is necessary to use EBC Methods 9.43.1 or 9.43.2 and 9.28.1
The determination of the net contents of bottles manufactured as measuring containers in a non-destructive way by means of a template, a gauge for ascertaining the actual liquid (and/or vacuity) level.
The instrumental estimation of Pasteurisation Units (PU’s) by determination of time and temperature and the calculation of Pasteurisation Units in order to control the pasteuriser performance. With computer based overall supervision of the complete packaging line, it is possible to provide control of the pasteuriser and other items of packaging line equipment in response to changes in the whole system. For example, in a packaging line of small containers, in conjunction with the use of variable speed drive of the transport system, it is possible to control transit time and temperature of the pasteuriser to ensure the correct level of heat treatment for each group of containers, as represented by a line of containers across the width of the machine. Pasteurisation is a gentle heat treatment to reduce the microbial load in a product so that there is no micro-biological growth during shelf-life. Descriptors: Time required from a temperature of 60 °C until the product leaves the regeneration section of the plate heat exchanger in min, Outlet temperature of the regeneration section in °C, Time the product needs to go through the heating section of the plate heat exchanger in min, Temperature in holding loop in °C, Time in holding loop in min or Time the product needs to go through the holding loop in min, Time required for the product to reach 60 °C from the outlet of the holding loop to the regeneration section of the plate heat exchanger in min, Volume of holding tube in m3, Flow in m3/minute, Minimum temperature in holding loop in ° C, Pasteurisation temperature in °C
It is necessary to use ......
The determination of the total (the dissolved and the headspace) content of oxygen in packaged beer, in bottle, can, keg and cask, by means of detecting oxygen ingress during packaging transfer and filling. Descriptors: headspace volume, net content, correlation between the oxygen content of a liquid phase and of a gas phase at equilibrium, temperature of the sample in degrees K, reading of the oxygen meter in mg/litre or ug/l, conversion of the headspace ratio.
It is necessary to use EBC Methods 9.37, 11.3.2, 11.3.1, 11.27, 11.14 and 11.18
The determination of differentiated total package oxygen in packaged beer. Descriptors: HSO (Headspace Oxygen), headspace pressure, headspace volume, TPO (Total Package Oxygen), DO (Dissolved Oxygen), beer
The detection of the phosphatase enzyme, present in alleged insect contaminants. The method is based upon the Aschaffenburg and Mullen test for phosphatase in milk.
A biochemical assay for the presence or absence of the invertase enzyme as a measure of the effectiveness of pasteurisation, measured as pasteurisation units (PU). Other biochemical assays allow for quantitative measures of pasteurisation activity (see clause 9).
The checking of one-way container (cans, non-returnable glass and PET bottles,…) clean efficiency by analysis of cleaned one-way containers, which have been deliberately contaminated.
The determination of sodium hydroxide and aluminates in packaging container (bottles, kegs, casks) washing solutions. A correction for the effect of residual carbonate is described.
Assessment of caustic detergent carry over in bottle washers.
For the approval of new packaging materials or new suppliers by evaluating the aroma and taste of beer for potential taints. For use within problem solving related to off-flavours or taints.
It is necessary to use EBC Methods 13.14 and 13.3